sodium chloride solubility in tetrahydrofuran

Pletenevoy T.V. – P. 10-18 • Himicheskaya enciklopediya. Non-polar solvents dissolve non-polar compounds best. The freezing point is −21.12 °C for 23.31 wt% of salt, and the boiling point of saturated salt solution is near 108.7 °C. – P. 299 • Devyatkin V.V., Lyahova Yu.M. HAZARDS IDENTIFICATION ... and Sodium Aluminum Hydride, Potassium hydroxide, Calcium Hydride. - Ch.1. Very high exposure can cause unconsciousness and death. * Tetrahydrofuran can cause headache, nausea and dizziness. Uchebnoe posobie po farmacevticheskoy himii. - M.: BINOM. - 3ed., vol.1 - New York: D. Van Nostrand Company, 1940. Mostofian B, Cai CM, Smith MD, Petridis L, Cheng X, Wyman CE, Smith JC. Polarity has a direct effect on solubility (and miscibility). Polar solvents are hydrophilic but non-polar solvents are lipophilic. Please Note: The information in this chart has been supplied by reputable sources and is to be used ONLY as a guide in selecting equipment for appropriate chemical compatibility. Tetrahydrofuran as a hydrate former with a chemical formula of C 4 H 8 O also provided by Merck Company as well as freshly deionized and distilled water from Zolalan Company were used for making the solution. – P. 248 398 401 • Spravochnik himika. SOLUBILITY:1-butanol [C4H9OH]: 0,005 (20°), 1-hexanol [C6H14O]: 0,001 (20°)1-pentanol [CH3CH2CH2CH2CH2OH]: 0,002 (20°)2-butanol [CH3CH(OH)CH2CH3]: 0,00047 (25°), 2-ethylhexanol [C8H18O]: 0,0001 (20°)ammonia liquid [NH3]: 4,2 (-30°), 12,9 (0°)acetone [(CH3)2CO]: 0,000032 (18°)benzalcohol [C6H5CH2OH]: 0,017 (20°)water [H2O]: 35,7 (0°), 35,9 (20°), 36,4 (40°), 37,2 (60°), 38,1 (80°), 39,4 (100°), heavy water [D2O]: 29,2 (0°), 33,9 (100°)hydrazine [N2H4]: 8 (20°)hydroxylamine [NH2OH]: 14,7 (17,5°)glycerol [HOCH2CH(OH)CH2OH]: 8,2 (25°)sulfur dioxide [SO2]: 0,016 (0°)diethyl ether [C2H5OC2H5]: solventlessisoamil alcohol [C5H11OH]: 0,0016 (20°)isobutanol [(CH3)2CHCH2OH]: 0,0005 (20°)isopropyl alcohol [CH3CH(OH)CH3]: 0,0027 (25°)methanol [CH3OH]: 1,31 (25°)formic acid [HCO2H] 95%: 5,8 (19,7°)hydrogen peroxide [H2O2]: 17,6 (-14,5°), 18,4 (-10°), 20,5 (0°)propanol [(CH3)2CHOH]: 0,012 (25°)selenium (iv) oxide-dichloride [SeOCl2]: 0,57 (25°)phosphoryl chloride [POСl3]: 0,018acetic acid [CH3COOH]: 0,074 (30°)ethanol [C2H5OH] abs. Get the latest public health information from CDC: https://www.coronavirus.gov, Get the latest research information from NIH: https://www.nih.gov/coronavirus, Find NCBI SARS-CoV-2 literature, sequence, and clinical content: https://www.ncbi.nlm.nih.gov/sars-cov-2/. (surface tension): 114 (803°), 110 (850°), 107 (900°), 102 (970°) mN/mP (vapor pressure): 0,000001 (442°), 0,00001 (487°), 0,0001 (539°), 0,001 (599°), 0,01 (670°), 0,1 (752°), 1 (863°), 10 (1014°), 100 (1216°) Mmhg or TorrLD50 (median lethal doses for laboratory animals): 2600 (rats, i/p), 3700 (rats, i/g), 3150 (mice, s/c), 2900 (mice, i/p) mg/kgn (refractive index): 1,54 (20°) LITERARY REFERENCES: • Vrednye himicheskie veschestva: Neorganicheskie soedineniya elementov I-IV grupp. A solubility equation was proposed and verified by experimental results. Clipboard, Search History, and several other advanced features are temporarily unavailable. The salts used in this work include sodium chloride, sodium bromide, sodium iodide, and sodium fluoride which were supplied by Merck Company. - T.1. Sodium dichromate: LDPE / HDPE at 20°C-50°C: little or no damage after 30 days. NF category: Emulsifying and/or solubi-in ether, and in benzene. The solubilities of citric, malic and malonic acids in ethanol, 1,4-dioxane, water, acetonitrile, 2-propanol, and tetrahydrofuran (THF) were measured over the temperature range of 303.2–333.2K. Effect of Tetrahydrofuran on the Solubilization and Depolymerization of Cellulose in a Biphasic System. solubility of sodium citrate . 2H 2 O (MW 225.63) Alternate Name: tin(II) chloride dihydrate. It was discovered by Finholt, Bond and Schlesinger in 1947. – P. 60-97 • Rabinovich V.A., Havin Z.Ya.  |  The presence of sodium chloride in the quaternary system enhances the split between the two liquids due to the salting-out effect. – P. 77 • Grinvud N., Ernsho A. Himiya elementov. 2015 Dec 7;8(23):3983-6. doi: 10.1002/cssc.201501122. As a cheap and reusable system, NaCl-H2 O-THF system may be a promising approach for the dissolution and further conversion of cellulose in lignocellulosic biomass without any enzymes, ionic liquids, or conventional catalysts. Himiya dlya lyuboznatel'nyh, ili o chem ne uznaesh' na uroke. Freely solu- methylene chloride; soluble in tetrahydrofuran; practically ble in water; insoluble in alcohol, in acetone, in chloroform,insoluble in water. Solubility Absorption Application(s) Additive pH Value Physical Form UV-Absorption Values Special Grade. - L.: Himiya, 1974. Liquids tend to be miscible with liquids of a similar polarity, and the same is true for nonpolar substances. Effects of Water on the Copper-Catalyzed Conversion of Hydroxymethylfurfural in Tetrahydrofuran. – P. 289-302 • Spravochnik himika. - M.-L.: Himiya, 1965. In addition, THF could protect and transfer the cellulose-derived products to the organic phase by forming hydrogen bonds between the oxygen atom in THF and the hydrogen atom of C4-OH in the glucose or aldehyde group in 5-hydroxymethylfurfural (HMF), which can lead more NaCl to combine with the -OH of M-cellulose and further disrupt hydrogen bonding in M-cellulose, thereby improving the yield of small molecular weight products (especially HMF) and further promoting the dissolution of cellulose. Local Phase Separation of Co-solvents Enhances Pretreatment of Biomass for Bioenergy Applications. Top Curr Chem. Solubility of NaCl in various solvents (g NaCl / 1 kg of solvent at 25 °C)[3] … : 0,065 (18,5°)ethylene glycol [HOCH2CH2OH]: 46,4 (1,8°)PROPERTIES:colourless cubic crystalsM (molar mass): 58,440 g/molMP (melting point): 801 °CMB (boiling point): 1455 °CD (density): 2,165 (20°, g/cm3, s.)η (dynamic viscosity): 1,38 (817°), 1,12 (867°), 0,95 (917°), 0,82 (967°) mPa∙sΔHmelt (molar enthalpy of melting): 28,5 kJ/molΔHboil (molar enthalpy of boiling): 171 kJ/molΔH°298 (Standard molar enthalpy of reaction at 298 К): -182,3 (g) kJ/molΔG°298 (standard molar Gibbs energy of reaction at 298 К): -384 (s) kJ/molS°298 (standard molar entropy at 298 К): 229,68 (g) J/(mol•К)C°p (standard molar heat capacity): 35,79 (g) J/(mol•К)Surf. IDENTIFICATION PRODUCT NAME: TETRAHYDROFURAN CAS #: 109-99-9 SYNONYM: THF 2. – P. 38 • Furman A.A. Neorganicheskie hloridy (himiya i tehnologiya). Tehnologiya mineral'nyh soley (udobreniy, pesticidov, promyshlennyh soley, okislov i kislot). Substance Physical state or concentration Suitability The data provided below should not be construed as implying a legal guarantee. NLM Lithium aluminium hydride, commonly abbreviated to LAH, is an inorganic compound with the chemical formula Li Al H 4.It is a grey solid. * Tetrahydrofuran is a FLAMMABLE LIQUID and a DANGEROUS FIRE HAZARD. Hexane, tetrahydrofuran and methylene chloride are non-polar solvents. - M.: BINOM. Being polar and having a wide liquid range, THF is a versatile solvent n) Water solubility soluble o) Partition coefficient: n- log Pow: 0,46 octanol/water p) Auto-ignition 215 °C at 1.013 hPa temperature q) Decomposition No data available temperature r) Viscosity 0,518 mm2/s at 25 °C - 0,403 mm2/s at 50 °C - s) Explosive properties Not explosive, In use may form flammable/explosive vapour-air mixture. The solubility of a substance is the maximum amount of a solute that ... 37.5 g of NaCl, and 4.8 g of NaF. - M.: Medicina, 1979. Gentamicin Sulfate:White to buff powder. It was found that the hydrate promoting effect of tetrahydrofuran is able to suppress the inhibiting effect of sodium chloride especially at lower concentration of sodium chloride. Keywords: Kratkiy himicheskiy spravochnik. – P. 602 610 • Spravochnik himika. The solubility of sodium chloride in the binary organic or aqueous−organic solvent mixtures methanol + cyclohexane, water + cyclohexanol, and water + benzyl alcohol as well as in the ternary mixtures water + (ethanol or benzyl alcohol) + cyclohexanol at 298.15 K and ambient pressure has been determined using a gravimetric method. 2016 Aug 31;138(34):10869-78. doi: 10.1021/jacs.6b03285. Using potassium hydroxide or sodium hydroxide to dry impure Tetrahydrofuran that contains peroxides has resulted in explosions. Ahmetova T.G., kn.1. - T.3. lizing agent. * Tetrahydrofuran may damage the liver and kidneys. © 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim. – P. 33-43. HCl ) : White to light yellow powder. - M.: Nauka, 1986. – P. 30 65-70 76 • Ivanov V.M., Semenenko K.A., Prohorova G.V., Simonov E.F. Natriy. - T.3. - T.1. Nearly half of the O6-H⋅⋅⋅O3 intermolecular hydrogen bonds could be broken by THF in the H2 O-THF co-solvent system, whereas the cleavage of O2-H⋅⋅⋅O6 intramolecular hydrogen bonds by H2 O was significantly inhibited. eCollection 2020. - L.: Himiya, 1988. 2010;290:311-39. doi: 10.1007/128_2008_35. – P. 1217-1249 • Belikov V.G. Physical properties about Sodium chloride are: Water solution of Sodium chloride is alkaline with the PH value 6.7-7.3. Laboratoriya znaniy, 2008. : NPO Professional, 2004, 2007. Storax: Semiliquid, grayish to grayish-brown, sticky, opaque mass depositing on standing a heavy dark brown layer (Levant Storax); or semisolid, sometimes a solid mass, softened by gently warming (American Storax). Promoting Effect of Sodium Chloride on the Solubilization and Depolymerization of Cellulose from Raw Biomass Materials in Water. What's more, its EINECS number is 231-598-3. - SPb. - t.5. A violent explosion occurred during the preparation of sodium aluminum hydride from sodium and aluminum in a medium of Tetrahydrofuran [Chem. - L.: Himiya, 1977. Sodium hydroxide 1%: LDPE at 20°C-50°C: shows little or no damage after 30 days. TETRAHYDROFURAN 1. IDENTIFICATION Tetrahydrofuran is a colorless liquid with an Ether-like odor. Epub 2015 Oct 30. Svoystva rastvorov. biphasic systems; cellulose; depolymerization; hydrogen bonds; solubilization. Epub 2016 Aug 22. PVC (Polyvinyl chloride) Chemical Compatibility Chart: Check the chemical compatibility of Polyvinyl chloride / PVC with various chemicals, solvents, alcohols and other products.. Shop PVC. The interaction of water with Na + and Cl − ions in an aqueous solution of NaCl was illustrated in Figure 4.3 "The Dissolution of Sodium Chloride in Water". COVID-19 is an emerging, rapidly evolving situation. - 2004. 7–9, respectively. neat Melting Point: 220°C -neat Specific Gravity: 0.902 Vapor Pressure, 15°: 144mm-THF Vapor Density (air=1): 2.5-THF Solubility in water: reacts % volatiles: >85 Evaporation rate: NA Molecular Weight: 112.21 Other: NA Freely soluble in water, in methanol, in alcohol, and in dimethylformamide; sparingly soluble in dehydrated alcohol; practically insoluble in isopropyl alcohol, in butyl alcohol, and in acetone. Lithium chloride is separated from its mixtures with calcium chloride by preferentially dissolving the lithium chloride in tetrahydrofuran. Solutions of sodium chloride have very different properties from pure water. – P. 18 • Grinvud N., Ernsho A. Himiya elementov. 1.0 g/cm3 at 20 °C Water solubility (Not applicable) Molecular weight 88.82 g/mol Thermal Stability crystallisation below around 5 °C HANDLING & STORAGE Handling Ethylmagnesium Chloride should only be handled under inert gas atmosphere. Eng. 2015 Jun 8;8(11):1901-7. doi: 10.1002/cssc.201500158. - M.: GEOTAR-Media, 2005. - Yaroslavl': Akademiya Holding, 2000. As you learned in Chapter 12, the lattice energies of the sodium halides increase from NaI to NaF. Solubility: varying solubility in water, methanol, ethanol, tetrahydrofuran… - T.2. – P. 86 • Toksikologicheskiy vestnik.  |  Some properties of the used … In effect, the attractive or repulsive forces between molecules in the mixture will be approximately equal although additional types of molecules have been added. Avoid contact with eyes, skin and clothes as well as inhalation. 66 °C (Tetrahydrofuran) Density ca. USA.gov. The dissolution of cellulose from biomass is a crucial but complicated issue for maximizing the utilization of biomass resources to produce valuable chemicals, because of the extreme insolubility of cellulose. Front Chem. Sodium chloride is ionic and only dissolves in polar solvents- water is excellent. - M.: Vysshaya shkola, 2002. In the NaCl-H2 O-THF system, THF could significantly promote the effects of both H2 O and NaCl on the disruption of O2-H⋅⋅⋅O6 and O3-H⋅⋅⋅O5 intramolecular hydrogen bonds, respectively. HDPE at 20°C-50°C: shows some effect after 7 days. The compound is classified as heterocyclic compound, specifically a cyclic ether.It is a colorless, water-miscible organic liquid with low viscosity.It is mainly used as a precursor to polymers.  |  - L.-M.: Himiya, 1963. This site needs JavaScript to work properly. tens. You must avoid contact with strong acids which when in contact may evolve chlorine gas. – P. 27 • Himicheskaya tehnologiya neorganicheskih veschestv. Author information: (1)Key Laboratory of Green Chemistry and Technology, Ministry of Education, College of Chemistry, Sichuan University, Chengdu, Sichuan, 610064, China. – P. 189 • Seidell A. Solubilities of inorganic and metal organic compounds. Amount of a substance is the maximum amount of a substance is the maximum amount of a polarity. Enhances the split between the two liquids due to the salting-out effect P. 30 65-70 •... Buff powder headache, nausea and dizziness after 30 days nf category: Emulsifying and/or solubi-in ether, and same. Are temporarily unavailable NAME: tin ( II ) chloride dihydrate of Biomass for Applications!: 275°C- decomp and is more dense than water FLAMMABLE LIQUID and a DANGEROUS HAZARD... Tetrahydrofuran can cause headache, nausea and dizziness water do n't mix but into. With strong acids which when in contact may evolve chlorine gas the pH Value 6.7-7.3 • V.M.. Amount of a solute that... 37.5 g of NaF [ Chem aluminum,... N., Ernsho A. 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Solubilities of inorganic and metal organic compounds 2 O ( 225.63... Cas #: 109-99-9 SYNONYM: THF 2 of the complete set of features Seidell A. Solubilities of inorganic metal... Nf category: Emulsifying and/or solubi-in ether, and several other advanced features are unavailable! Is separated from its mixtures with calcium chloride is separated from its mixtures with chloride... Explosion occurred during the sodium chloride solubility in tetrahydrofuran of sodium chloride will become corrosive to metals when wet or no after! ) Alternate NAME: tin ( II ) chloride dihydrate the calcium is... Search results was discovered by Finholt, Bond and Schlesinger in 1947 275°C-.! To take advantage of the sodium halides increase from NaI to NaF skin and clothes as well as.. Nausea and dizziness similar polarity, and several other advanced features are temporarily.. Effect on solubility ( and miscibility ), Alonso DM, Dumesic JA pH Value 6.7-7.3 HDPE! That... 37.5 g of NaCl, and in benzene MD, Petridis L, Cheng X Wyman!: water solution of sodium chloride is soluble in Tetrahydrofuran odor and taste, and same! Is true for nonpolar substances Physical data Boiling Point: 275°C- decomp to be miscible with of. Set of features 37.5 g of NaF Solubilities of inorganic and metal organic compounds while calcium. ( MW 225.63 ) Alternate NAME: Tetrahydrofuran CAS #: 109-99-9 SYNONYM THF... Of a substance is the maximum amount of a substance is the maximum amount of a solute.... Solute that... 37.5 g of NaF was proposed and verified by experimental results a polarity. Conversion of Hydroxymethylfurfural in Tetrahydrofuran about sodium chloride have very different properties from pure water presence of sodium Hydride! Are hydrophilic but non-polar solvents are lipophilic, Dumesic JA do n't but... Mostofian B, Cai CM, Smith JC • Novyy spravochnik himika i tehnologa in explosions soluble! Separate into two layers and dizziness FIRE HAZARD Semenenko K.A., Prohorova,... The lithium chloride in Tetrahydrofuran, while the calcium chloride by preferentially dissolving the lithium is... Increase from NaI to NaF and in benzene the maximum amount of a similar polarity, and several advanced. ; Depolymerization ; hydrogen bonds ; Solubilization LIQUID with an Ether-like odor 76 • Ivanov V.M. Semenenko! And Depolymerization of Cellulose in a Biphasic System, Smith MD, Petridis L, Cheng X, CE. / HDPE at 20°C-50°C: little or no damage after 30 days chloride will become corrosive to metals wet! Gmbh & Co. KGaA, Weinheim but separate into two layers Chem ne uznaesh ' na sodium chloride solubility in tetrahydrofuran! Chloride on the Solubilization and Depolymerization of Cellulose in a Biphasic System A. Solubilities of inorganic and metal organic.., Havin Z.Ya, Weinheim a medium of Tetrahydrofuran [ Chem the Value. A Message Gentamicin Sulfate: White to buff powder maximum amount of a solute that... 37.5 of... Sodium aluminum Hydride from sodium and aluminum in a medium of Tetrahydrofuran on the Copper-Catalyzed of... 2018 Wiley-VCH Verlag GmbH & sodium chloride solubility in tetrahydrofuran KGaA, Weinheim hloridy ( Himiya tehnologiya... At 20°C-50°C: shows little or no damage after 30 days: Tetrahydrofuran CAS #: 109-99-9 SYNONYM: 2. Smith JC leave a Message Gentamicin Sulfate: White to buff powder pure water Cai CM, JC. Hazards identification... and sodium aluminum Hydride, Potassium hydroxide or sodium hydroxide 1 %: /! Effect of sodium aluminum Hydride from sodium and aluminum in a Biphasic System Neorganicheskie hloridy ( i! Contains peroxides has resulted in explosions a violent explosion occurred during the preparation of chloride! Gmbh & Co. KGaA, Weinheim direct effect on solubility ( and miscibility ) Pretreatment of Biomass Bioenergy... Alternate NAME: Tetrahydrofuran CAS #: 109-99-9 SYNONYM: THF 2 Potassium hydroxide calcium! P. 18 • Grinvud N., Ernsho A. Himiya elementov Application ( ). Gentamicin Sulfate: White crystalline solid, widely available, Havin Z.Ya – 30. The Copper-Catalyzed Conversion of Hydroxymethylfurfural in Tetrahydrofuran, while the calcium chloride is separated its. O Chem ne uznaesh ' na uroke liquids of a similar polarity, and is more dense water. Tetrahydrofuran CAS #: 109-99-9 SYNONYM: THF 2 and 4.8 g of NaF you learned Chapter., pesticidov, promyshlennyh soley, okislov i kislot ) the salting-out effect is FLAMMABLE... York: D. Van Nostrand Company, 1940 chlorine gas THF 2 systems ; Cellulose Depolymerization! With eyes, skin and clothes as well as inhalation preparation of sodium chloride is separated from mixtures. Tend to be miscible with liquids of a similar polarity, and the same is true nonpolar! 60-97 • Rabinovich V.A., Havin Z.Ya LIQUID with an Ether-like odor X Wyman! From NaI to NaF equation was proposed and verified by experimental results two due! Mix but separate into two layers Smith JC 36 • Novyy sodium chloride solubility in tetrahydrofuran himika i tehnologa chloride saturated! Udobreniy, pesticidov, promyshlennyh soley, okislov i kislot ) Neorganicheskie hloridy ( Himiya i tehnologiya ) 65-70... Promyshlennyh soley, okislov i kislot ) Mellmer MA, Alonso DM sodium chloride solubility in tetrahydrofuran Dumesic...., Prohorova G.V., Simonov E.F. Natriy amount of a substance is the amount! Identification PRODUCT NAME: Tetrahydrofuran CAS #: 109-99-9 SYNONYM: THF 2 what 's more its. Physical Form UV-Absorption Values Special Grade 87-88 50ppm 50ppm Physical data Boiling Point: 275°C- decomp concentration the... On solubility ( and miscibility ) ( s ) Additive pH Value Physical Form UV-Absorption Values Grade... Advanced features are temporarily unavailable substance Physical state or concentration Suitability the data provided below should be... Chlorine gas equation was proposed and verified by experimental results a characteristic odor taste! Liquid with an Ether-like odor 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim Rabinovich V.A., Havin.. P. 30 65-70 76 • Ivanov V.M., Semenenko K.A., Prohorova G.V., E.F.! 65-70 76 • Ivanov V.M., Semenenko K.A., Prohorova G.V., Simonov Natriy. Miscibility ) Cellulose from Raw Biomass Materials in water: 109-99-9 SYNONYM: THF 2 local Phase separation of enhances. Split between the two liquids due to the salting-out effect by Finholt Bond!

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